Otorhinolaryngology
- Cervical presentation of tracheal diverticulum: From diagnosis to surgeryPublication date: Available online 27 September 2019Source: European Annals of Otorhinolaryngology, Head and Neck DiseasesAuthor(s): C. Maquet, S. Caluraud, E. De Sevin, N. Bon Mardion
- Persistent peripheral facial nerve palsyPublication date: Available online 27 September 2019Source: European Annals of Otorhinolaryngology, Head and Neck DiseasesAuthor(s): T.-T. Trinh, C. Dorbeau, C. Philibert, E. Lescanne
- Influence of surgical technique on residual cholesteatoma location and prevalencePublication date: Available online 26 September 2019Source: European Annals of Otorhinolaryngology, Head and Neck DiseasesAuthor(s): P. Rayneau, C. Aussedat, T.T. Trinh, C. Bobillier, E. Lescanne, A. Robier, D. BakhosAbstractObjectiveCompared to canal wall up (CWU) tympanoplasty, canal wall reconstruction (CWR) allows better visualization of cholesteatoma extension. The canal wall up approach provides good functional outcomes, but with higher rat
Journal of Voice
- Voice Outcome of Total Thyroidectomy in Comparison With Administration of Recombinant Human TSHThe larynx is an end-organ target for hormones, and thyroid hormone may act on the larynx. We objectively compared and analyzed the phonetic characteristics of patients who underwent total thyroidectomy before and after radioiodine therapy (RIT) according to administration of recombinant human TSH (rh-TSH).
Medgadget
- Artificial Skin to Improve Sense of Touch, Help Study Neural ActivityAt the Ecole polytechnique fédérale de Lausanne (EPFL) in Switzerland, researchers have created an interesting artificial “skin” that can sense touch while providing real-time haptic feedback in the form of vibrations. Because the sensors and actuators are completely embedded within this skin, it allows for near simultaneous closed-loop control of the system and makes it usable for a variety of rehab, research, as well as virtual reality and gami
- Samsung Unveils Hera I10 Ultrasound SystemSamsung is unveiling its new Hera I10 ultrasound system designed for ob/gyn applications. The system integrates a motorized examination chair that can adjust from 18.9″ to a height of 38.6″, so patients don’t have to put up with a conventional exam table. A large high-def display screen can be moved around as the clinician prefers it, helping to increase productivity and improve ergonomics. On the side is a convenient rack
- Light Activated Compound Kills Hypoxic TumorsPhotodynamic therapy is a technique that relies on photosensitizer chemicals to generate reactive species that kill cancer cells. These compounds can be delivered into tumors and then light is used to activate them. One of the main reasons for the slow adoption of this technology is that tumors are usually oxygen deprived and the photosensitizers developed to date require the presence of copious amounts of oxygen. Now, an international tea
Angewandte Chemie International Edition
- Visible light driven Janus microvehicles in biological mediaA multi‐light (bio)‐driven multifunctional Janus micromotor for the enhanced (bio)‐detoxification of bacterial endotoxins and heavy metals is described. The micromotor is assembled using the highly biocompatible polymer polycaprolactone for the encapsulation of CdTe or CdSe@ZnS quantum dots (QDs) as photoactive materials and an asymmetric Fe3O4 patch for propulsion. The micromotors can be activated by visible light (470‐490 nm) to propel in perox
- Extraordinary Enhancement of π‐Electron Donor/Acceptor Ability by DD/AA Complementary Hydrogen Bondingπ‐Conjugated organic materials possess a wide range of tunable optoelectronic properties which give rise to many device applications. These properties are dictated by their molecular structure and their supramolecular arrangement. While much efforts in the past decades have been put into tuning the molecular structure to achieve desired properties, rational supramolecular control remains a challenge. Here we report a novel series of supramolecula
- Nucleophilicity of Glutathione: A Link to Michael Acceptor ReactivitiesDeprotonated glutathione is among the most potent biological nucleophiles and plays an important physiological role in cellular detoxification by forming covalent conjugates with Michael acceptors. The electrophilicity E of various Michael acceptors was characterized recently according to the Patz‐Mayr relation lg k 2 = s N ( N + E ). We now determined the nucleophilic reactivity ( N , s N ) of glutathione (GSH) in aqueous soluti
- Controlled Growth of CH₃NH₃PbBr₃ Perovskite Nanocrystals via a Water‐Oil Interfacial Synthesis MethodFundamental insights into the reaction kinetics of organic‐inorganic lead halide perovskite nanocrystals (LHP NCs) are still limited due to their ultrafast formation rate. Herein, we develop a water‐oil interfacial synthesis of MAPbBr₃ NCs, which prolongs the reaction time to tens of minutes. This method makes it possible to in situ monitor the formation process of MAPbBr₃ NCs and observe successive spectral evolutions from 438 to 534 nm in a sin
- Orthogonal Nanoparticle Catalysis with OrganogermaniumsAlthough nanoparticles are widely used as catalysts, little is known about their potential ability to trigger privileged transfor‐mations as compared to homogeneous molecular or bulk heterogeneous catalysts. We herein demonstrate (and rationalize) that nanoparticles display orthogonal reactivity to molecular catalysts in the cross‐coupling of aryl halides with aryl germanes. While the aryl germanes are unreactive in LnPd(0)/LnPd(II) catalysis and
- Identifying Copper Vacancies and their Role in CuO based Photocathodes for Water SplittingMetal oxides represent an important family of semiconductors for fabricating effective photoelectrodes in solar‐to‐chemical energy conversion application. Defect engineering such as modification of oxygen vacancy density has been widely studied in tailoring the optoelectronic properties of photelectrodes, but very limited attention has been paid to the influence of metal vacancies. In this work, we focus on the understanding of metal vacancies in
- Dopant‐free Squaraine‐based Polymeric Hole Transporting Materials with Comprehensive Passivation effect for Efficient All‐inorganic Perovskite Solar CellsDevelopment of high performance dopant‐free hole transporting materials (HTMs) with comprehensive passivation effect is highly desirable for all‐inorganic perovskite solar cells (PVSCs). Squaraines (SQs) could be one of ideal material candidates of dopant‐free HTMs as they are natural passivators for perovskites. One major limitation for SQs to be efficient dopant‐free HTMs is their relatively low hole mobilities. Herein we demonstrate that polym
- Multiple Anti‐counterfeiting Guarantees from a Simple Tetraphenylethylene Derivative —— High‐contrasted and Multi‐state Mechanochromism and PhotochromismHerein a novel tetraphenylethylene (TPE) derivative 1 was designed with an integration of aggregation‐induced emission (AIE), multi‐state mechanochromism and self‐recovery photochromism. The molecule was susceptible to grinding, heating and vapor fuming and showed corresponding transition of its emission colors. The heated powder or single crystal of 1 exhibited reversible photochromism: when a short period of UV irradiation was turned off, i
- Efficient Non‐dissociative Activation of Dinitrogen to Ammonia over Li Promoted Ru Nanoparticles at Low PressureThere is an exciting possibility to decentralize ammonia synthesis for fertilizer production or energy store without carbon emission from H2 obtained from renewables at small units operated at lower pressure. However, no suitable catalyst is yet developed. Ru catalysts are known to be promoted by heavier alkali dopants. Instead of using higher alkali metals down in periodic table, Li is hereby found to give the highest rate due to surface polaris
- Large‐Area Synthesis of Superclean Graphene via Selective Etching of Amorphous Carbon with Carbon DioxideSpic and span! A facile and scalable chemical vapor deposition approach was developed to synthesize meter‐sized samples of superclean graphene with an average cleanness of 99 %. The weak oxidizing ability of CO2 was essential to selectively etch away the intrinsic contamination, amorphous carbon, on the graphene surface. Abstract Contamination commonly observed on the graphene surface is detrimental to its excellent properties and strongly
- Computationally Driven Discovery of a Family of Layered LiNiB PolymorphsBy design: Novel lithium nickel borides with unique layered structures were theoretically predicted and synthesized. Their structures are composed of [NiB] layers with different topologies alternating with layers of Li cations (see picture). These compounds are ultimate precursors for further exfoliation to generate 2D transition‐metal borides, known as MBenes. Abstract Two novel lithium nickel boride polymorphs, RT‐LiNiB and HT‐LiNiB, with
- Organic Room Temperature Phosphorescence with Strong Circular Polarized Luminescence based on ParacyclophanesPure organic materials with intrinsically ultralong room temperature phosphorescence characteristics are a unique category which typically relies on heavy atoms or heteroatoms. In this study, two different strategies towards constructing organic room temperature phosphorescence (RTP) species based upon the through‐space charge transfer (TSCT) unit of [2.2]paracyclophane (PCP) were demonstrated for the first time containing bromine, carbazole, pic
- Awakening Rhodium Catalysis for C–H Activation with an In‐MetalloligandRhodium complexes having an In‐metalloligand are successfully synthesized utilizing a pyridine‐tethered cyclopentadienyl ligand as a support for an In–Rh bond. The In‐metalloligand dramatically changes the electronic and redox properties of the rhodium metal, awakening its catalysis for an sp2C–H bond activation reaction.
- Butenolide Derivatives of Biobased Furans: Sustainable Synthetic DyesButenolide Derivatives of Biobased Furans: Sustainable Synthetic DyesThe dye and pigment manufacturing industry is one of the most polluting in the world. Each year, over one million tons of petrochemical colorants are produced globally, the synthesis of which generates a large amount of waste. Naturally occurring, plant‐based dyes, on the other hand, are resource intensive to produce (land, water, energy), and are generally less effective as colorants. Between these two extremes would be synthetic dyes that are f
- Defect‐Rich Adhesive Nanozymes as Efficient Antibiotics for Enhanced Bacterial InhibitionDefect‐rich, adhesive nanozymes: A rough surface endows nanozymes with the ability to trap bacteria and defect‐rich edges enhance their peroxidase‐like activity, increasing antibacterial activity in comparison to pristine nanozymes. Abstract Nanozymes have emerged as a new generation of antibiotics with exciting broad‐spectrum antimicrobial properties and negligible biotoxicities. However, their antibacterial efficacies are unsatisfactory d
- Universal Scaffold for an Activatable Photosensitizer with Completely Inhibited PhotosensitivityA long‐wavelength D‐π‐A photosensitizer (PS) with highly efficient photosensitivity for the generation of singlet oxygen (1O2) is used as the scaffold for activatable photosensitizers (aPSs). Caging of a phenolate donor provides a facile approach for preparing the aPS, as demonstrated intracellularly by the alkaline phosphatase activatable ALPPS and peroxynitrite‐activatable mito‐PNPS. Abstract Activatable photosensitizers (aPSs) sensitive
- An Ultrastable Matryoshka [Hf13] Nanocluster as a Luminescent Sensor for Concentrated Alkali and AcidTough beyond belief: An ultrastable Hf13(μ4‐O)8(OCH3)36 nanocluster (see picture; Hf green, O red, C gray) preserved its crystalline state in concentrated alkali (20 m boiling NaOH) and concentrated acid (10 m HNO3). The cluster acted as a luminescent sensor for the detection of both strong acid and concentrated alkali with high selectivity and repeatability. Abstract Stable metal clusters that can resist both highly concentrated acid and a
- Spontaneous Crystallization of Perovskite Nanocrystals in Nonpolar Organic Solvents: A Versatile Approach for their Shape‐Controlled SynthesisFaster than fast: Shape‐controlled lead halide perovskite nanocrystals crystallize spontaneously at ambient conditions when precursor–ligand complexes are mixed directly in a nonpolar organic medium. Nanocubes and nanoplatelets have been obtained. This versatile synthetic process is generally applicable for a wide range of halide perovskite nanocrystals. Abstract The growing demand for perovskite nanocrystals (NCs) for various applications
- Electrochemical Production of Si without Generation of CO2 Based on the Use of a Dimensionally Stable Anode in Molten CaCl2Make a deposit: A highly electrically conductive anode, Ti4O7, was applied in molten CaCl2‐CaO‐SiO2 and successfully produced elementary Si without any CO2 emissions. In situ or ex situ methods can be used to efficiently regenerate the anode and extend its lifetime. The deposited Si films show good photoelectrochemical properties. Abstract The current Si production process is based on the high‐temperature (1700 °C) reduction of SiO2 with ca
- Synergy of Epoxy Chemical Tethers and Defect‐Free Graphene in Enabling Stable Lithium Cycling of Silicon NanoparticlesEpoxy‐tethered nanosilicon–pristine graphene (E‐Si‐pG) hybrids with uniquely stable structure and solid electrolyte interphase (SEI) layer were prepared. The E‐Si‐pG anode exhibits excellent energy and cyclability in a full battery, opposing commercial mass loading LiCoO2 cathode. The key link between graphene defects, surface tethers and SEI is discovered. Abstract We report a new approach for nanosilicon–graphene hybrids with uniquely sta
- Interfacial Enhancement by γ‐Al2O3 of Electrochemical Oxidative Dehydrogenation of Ethane to Ethylene in Solid Oxide Electrolysis CellsThe interfacial interaction between the γ‐Al2O3 and the LSCF enhances ethane adsorption and selective conversion to ethylene by modifying the electronic structure of Fe center at the Al‐O‐Fe interface and decreasing surface adsorbed oxygen species. Abstract Oxidative dehydrogenation of ethane (ODE) is limited by the facile deep oxidation and potential safety hazards. Now, electrochemical ODE reaction is incorporated into the anode of a soli
- Combined Photoredox/Enzymatic C−H Benzylic HydroxylationsLight and enzymes: A strategy for chemoenzymatic catalysis combining photoredox catalysed oxidation and enzymatic reduction has been developed. This single‐flask process affords value‐added enantiomerically enriched benzylic alcohols across a wide variety of substrate classes. Abstract Chemical transformations that install heteroatoms into C−H bonds are of significant interest because they streamline the construction of value‐added small mo
- Crystal‐State Photochromism and Dual‐Mode Mechanochromism of an Organic Molecule with Fluorescence, Room‐Temperature Phosphorescence, and Delayed FluorescenceA pure organic D‐A‐D′ type molecule ODFRCZ is synthesized, which shows unique fluorescence–phosphorescence–delayed fluorescence (DF) triple‐emission character. It is a rare example of an organic room‐temperature phosphorescence (RTP) molecule showing dual‐stimuli responsiveness of reversible crystal‐state photochromism and dual‐mode mechanochromism of fluorescence red‐shift and RTP/DF on–off switching. Abstract A D‐A‐D′ type pure organic mo
- Synthesis of Tetraarylethene Luminogens by C−H Vinylation of Aromatic Compounds with TriazenesGlowing couple: A simple and versatile coupling method to make tetraarylethenes, which display active aggregation‐induced emission, from aromatic compounds and vinyl triazenes is described. The novel C−H vinylation approach allows installation of the triarylethenyl group onto simple unactivated arenes, heteroarenes, supramolecular hosts, bioactive molecules, and polymers. Abstract Tetraarylethenes are obtained by acid‐induced coupling of vi
- Electrolyte Chemistry Enables Simultaneous Stabilization of Potassium Metal and Alloying Anode for Potassium‐Ion BatteriesOf salts and solvents: Alloying anodes universally exhibit poor cycling performance for K‐ion storage due to the degradation of highly active K metal and the large volume expansion. Here, it is revealed that the regulation of electrolyte chemistry is a feasible approach to simultaneously stabilize K metal and alloying anodes for realizing high‐performance K‐ion batteries based on alloying anodes. Abstract Alloying anodes are promising high‐
- Hooking Together Sigmoidal Monomers into Supramolecular PolymersHooked! An approach to prepare supramolecular polymers by hooking together sigmoidal monomers into 1D arrays of π‐stacked anthracene and acridine units is presented. It gives rise to micrometer‐sized fibrils that show pseudoconductivities, in line with other conducting materials. Abstract Supramolecular polymers show great potential in the development of new materials because of their inherent recyclability and their self‐healing and stimul
- Redox‐State‐Mediated Regulation of Cytochrome c Release in Apoptosis Revealed by Surface‐Enhanced Raman Scattering on Nickel SubstratesBring a nickel, tap your feet: By using surface‐enhanced Raman spectroscopy on nickel substrates, it is shown that the redox‐state of cytochrome c regulates cytochrome c release from mitochondria in apoptotic cells. The SERS data and MD simulations show that the ferrous state of Cyt c most likely plays a more important role in triggering apoptosis. Abstract The interaction of cytochrome c (Cyt c) with cardiolipin (CL) is believed to play an
- Blue LED Irradiation of Iodonium Ylides Gives Diradical Intermediates for Efficient Metal‐free Cyclopropanation with AlkenesDoubly activated cyclopropanes are generated upon irradiating alkenes and β‐dicarbonyl‐derived iodonium ylides with visible light from blue LEDs. This metal‐free cyclopropane synthesis works with cyclic and acyclic ylides, and with electronically‐diverse alkenes, in yields up to 96 %. Computational analysis supports a mechanism based on exclusive HOMO to LUMO excitation, instead of free carbene generation. Abstract A facile and highly chemo
- Bifunctional Small‐Molecule Ligands of K‐Ras Induce Its Association with Immunophilin ProteinsBifunctional ligands are designed and synthesized that induce the association of K‐Ras and immunophilin proteins including FKBP12 and cyclophilin A. The recruitment of cyclophilin A to GTP‐bound Ras blocks its interaction with B‐Raf. Abstract Here we report the design, synthesis, and characterization of bifunctional chemical ligands that induce the association of Ras with ubiquitously expressed immunophilin proteins such as FKBP12 and cyclo
- Modulating Polymer Dispersity with Light: Cationic Polymerization of Vinyl Ethers Using Photochromic InitiatorsA light touch: The use of carboxy‐functionalized dithienylethene photochromes as initiators in controlled cationic polymerizations of vinyl ethers enables the photocontrol of polymer dispersity. Reversible photoisomerization of these initiators induces changes in their acidities by up to an order of magnitude, and the degree of light‐induced acidity change correlates with the degree of dispersity change. Abstract Deterministic methods for t
- Controlled Incorporation of Nitrides into W‐Fe‐S ClustersTwo synthetic strategies have been developed for installing monatomic 2p ligand into iron–sulfur clusters offering better mimicking of the FeMo cofactor structure. Nitride‐ligated W‐Fe‐S clusters have been synthesized for the first time, which also provide useful references for understanding reduced nitrogen in a mid‐valent nitrogenase‐like environment. Abstract Incorporation of monatomic 2p ligands into the core of iron–sulfur clusters has
- A Plasma‐Triggered O−S Bond and P−N Junction Near the Surface of a SnS2 Nanosheet Array to Enable Efficient Solar Water OxidationArgon plasma treatment was proposed to introduce SnS/SnS2 P−N heterojunctions and O−S bonds near the surface of a SnS2 nanosheet array, simultaneously increasing the separation efficiency of photogenerated electron–hole pairs in the bulk and lowering the OER overpotential at the surface. The plasma‐treated sample showed a seven times higher photocurrent than that of pristine SnS2. Abstract A photoelectrochemical (PEC) cell can split water i
- Shigeki Matsunaga“My first experiment was an epoxide ring opening with tBuSH. Reaction was partially successful, but the laboratory was filled with terrible smell … If I could be a piece of lab equipment, I would be a UV lamp for checking TLC …” Find out more about Shigeki Matsunaga in his Author Profile.
- Time‐dependent Photodynamic Therapy for Multiple Targets: A Highly Efficient AIE‐active Photosensitizer for Selective Bacterial Elimination and Cancer Cell AblationPathogen infection and cancer are the two major human health problems. In this work, we achieved an organic salt photosensitizer (PS), called 4TPA‐BQ with aggregation‐induced emission feature via one‐step reaction. Owing to the aggregation‐induced reactive oxygen species generation effect and sufficient small ΔE ST , 4TPA‐BQ shows a satisfactorily high 1 O 2 generation efficiency of 97.8%. In vitro and in vivo experiments confirmed th
- Self‐Assembly of Phosphate‐Centered Polyoxo‐Titanium Cluster: Discovery of New “Heteroatom Keggin Family”Over the past 200 years, the most famous and important “heteroatom Keggin architecture” in polyoxometalates is only synthesized by Mo, W, V or Nb element. Herein, we first report the self‐assembly of two phosphate (PO 4 3‐ )‐centered polyoxo‐titanium clusters (PTCs), PTi 16 and PTi 12 , which display classic heteroatom Keggin and its trivacant structures, respectively. Because Ti IV has lower oxidate state and larger ionic radius than
- Long‐lived azafullerenyl radical stabilized by supramolecular shielding with a [10]cycloparaphenyleneA major handicap towards exploitation of radicals is their inherently instability. In paramagnetic azafullerenyl radical C59N• the unpaired electron is strongly localized neighbouring the nitrogen and induces dimerization to diamagnetic bisazafullerene (C59N)2. Conventional stabilization employing steric hindrance around the radical is inapplicable due to the concave fullerene geometry. Instead, we develop an innovative radical shielding approach
- Multifunctional Tubular Organic Cage‐Supported Ultrafine Palladium Nanoparticles for Sequential CatalysisThe imine condensation reaction of 5,5'‐(benzo[c][1,2,5]thiadiazole‐4,7‐diyl)diisophthalaldehyde with cyclohexanediamine resulted in a shape‐persistent multifunctional tubular organic cage (MTC1). It exhibits selective fluorescence sensing towards divalent palladium ions with a very low detection limit of 38 ppb, suggesting the effective complexation between these two species. The subsequent reduction of MTC1 and palladium acetate with NaBH4 affo
ΩτοΡινοΛαρυγγολόγος Medicine by Alexandros G. Sfakianakis,Anapafseos 5 Agios Nikolaos 72100 Crete Greece,00302841026182,00306932607174,
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Κυριακή 29 Σεπτεμβρίου 2019
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Medicine by Alexandros G. Sfakianakis,Anapafseos 5 Agios Nikolaos 72100 Crete Greece,00302841026182,00306932607174,alsfakia@gmail.com,
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00302841026182,
00306932607174,
alsfakia@gmail.com,
Anapafseos 5 Agios Nikolaos 72100 Crete Greece,
Medicine by Alexandros G. Sfakianakis
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